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Experimental study on mechanical properties of a novel micro-steel fiber reinforced magnesium phosphatecement-based concrete

《结构与土木工程前沿（英文）》 2021年 第15卷 第4期   页码 1047-1057 doi: 10.1007/s11709-021-0755-3

摘要： Magnesium phosphate cement (MPC) received increased attention in recent years, but MPC-based concrete is rarely reported. The micro-steel fibers (MSF) were added to MPC-based concrete to enhance its ductility due to the high brittleness in tensile and flexural strength properties of MPC. This paper investigates the effect of MSF volume fraction on the mechanical properties of a new pattern of MPC-based concrete. The temperature development curve, fluidity, cubic compressive strength, modulus of elastic, axial compressive strength, and four-point flexural strength were experimentally studied with 192 specimens, and a scanning electron microscopy (SEM) test was carried out after the specimens were failed. Based on the test results, the correlations between the cubic compressive strength and curing age, the axial and cubic compressive strength of MPC-based concrete were proposed. The results showed that with the increase of MSF volume fraction, the fluidity of fresh MPC-based concrete decreased gradually. MSF had no apparent influence on the compressive strength, while it enhanced the four-point flexural strength of MPC-based concrete. The four-point flexural strength of specimens with MSF volume fraction from 0.25% to 0.75% were 12.3%, 21.1%, 24.6% higher than that of the specimens without MSF, respectively.

关键词： magnesium phosphate cement-based concrete     micro-steel fibers     four-point flexural strength     compressive strength    

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Autogenous healing mechanism of cement-based materials

《结构与土木工程前沿（英文）》   页码 948-963 doi: 10.1007/s11709-023-0960-3

摘要： Autogenous self-healing is the innate and fundamental repair capability of cement-based materials for healing cracks. Many researchers have investigated factors that influence autogenous healing. However, systematic research on the autogenous healing mechanism of cement-based materials is lacking. The healing process mainly involves a chemical process, including further hydration of unhydrated cement and carbonation of calcium oxide and calcium hydroxide. Hence, the autogenous healing process is influenced by the material constituents of the cement composite and the ambient environment. In this study, different factors influencing the healing process of cement-based materials were investigated. Scanning electron microscopy and optical microscopy were used to examine the autogenous healing mechanism, and the maximum healing capacity was assessed. Furthermore, detailed theoretical analysis and quantitative detection of autogenous healing were conducted. This study provides a valuable reference for developing an improved healing technique for cement-based composites.

关键词： autogenous healing     cement-based materials     healing mechanism     aggregation effect    

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Effect of size on biaxial flexural strength for cement-based materials by using a triangular plate method

Hakan T TURKER

《结构与土木工程前沿（英文）》 2022年 第16卷 第8期   页码 1017-1028 doi: 10.1007/s11709-022-0871-8

摘要： The effect of size on the biaxial flexural strength (BFS) of Portland cement mortar was investigated by using the recently proposed triangular plate method (TPM). An experimental program was conceived to study the size effect by keeping a constant water-cement ratio of 0.485, cement-sand ratio of 1:2.75, and using unreinforced triangular mortar plates of five different thicknesses and seven different side lengths. The BFS of the produced specimens was tested, and variations of BFS depending on specimen thickness and side length were determined. The results indicated that increases in triangular plate specimen side length and specimen thickness led to a decrease in the BFS of Portland cement mortar. The effect of specimen length increase on BFS was more significant than on the effect of the specimen thickness. The variations in specimens’ thickness indicated a deterministic Type I size effect, while the variations in specimens’ length showed an energetic-statistical Type I size effect.

关键词： testing     apparatus & methods     plain concrete     tensile properties     biaxial flexural strength     triangular plate method    

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Appraising the potential of calcium sulfoaluminate cement-based grouts in simulated permafrost environments

《结构与土木工程前沿（英文）》 2023年 第17卷 第5期   页码 722-731 doi: 10.1007/s11709-023-0950-5

摘要： The aim of this study is to appraise the potential of calcium sulfoaluminate (CSA) cement-based grouts in simulated permafrost environments. The hydration and performance of CSA cement-based grouts cured in cold environments (10, 0, and −10 °C) are investigated using a combination of tests, including temperature recording, X-ray diffraction (XRD) tests, thermogravimetric analysis (TGA), and unconfined compressive strength (UCS) tests. The recorded temperature shows a rapid increase in temperature at the early stage in all the samples. Meanwhile, results of the TGA and XRD tests show the generation of a significant quantity of hydration products, which indicates the rapid hydration of CSA cement-based grouts at the early stage at low temperatures. Consequently, the CSA cement-based grouts exhibit remarkably high early strength. The UCS values of the samples cured for 2 h at −10, 0, and 10 °C are 6.5, 12.0, and 12.3 MPa, respectively. The UCS of the grouts cured at −10, 0, and 10 °C increases continuously with age and ultimately reached 14.9, 19.0, and 30.6 MPa at 28 d, respectively. The findings show that the strength of grouts fabricated using CSA cement can develop rapidly in cold environments, thus rendering them promising for permafrost applications.

关键词： permafrost     low temperatures     calcium sulfoaluminate cement-based grouts     hydration reaction     compressive strength    

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高性能多功能水泥基复合材料 Article

Victor C. Li

《工程（英文）》 2019年 第5卷 第2期   页码 250-260 doi: 10.1016/j.eng.2018.11.031

摘要：

混凝土是一种不断发展的材料，甚至高性能混凝土的定义也正随着时间的推移而发生变化。本文所说的混凝土材料的高性能特性是指那些直接影响我们生活质量的民用基础设施的理想耐久性、回弹性和可持续性的特性。这些特性包括拉伸延展性、自体裂缝宽度控制和材料的“绿色”环保性。此外，智能功能应旨在通过响应结构周围环境的变化来提高基础设施的耐久性、回弹性和可持续性以实现其理想功能，从而使材料的行为方式更类似于某些生物材料。本文基于工程水泥基复合材料（ECC）的最新研究进展，提出可以设计出具有高性能兼智能多功能性的混凝土材料，并且其具有满足 21 世纪民用基础设施预期需求的潜力。本文重点介绍了 ECC 的相关特性以及未来研究的方向。

关键词： 高性能混凝土     多功能     智能     水泥基复合材料     耐久性     回弹性     可持续性     基础设施    

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Microbial self-healing of cracks in cement-based materials and its influencing factors

《结构与土木工程前沿（英文）》 doi: 10.1007/s11709-023-0986-6

摘要： Cement-based materials are brittle and crack easily under natural conditions. Cracks can reduce service life because the transport of harmful substances can cause corrosion damage to the structures. This review discusses the feasibility of using microbial self-healing agents for crack healing. Tubular and spherical carriers can be used to load microbial self-healing agents and protect microbes, which prolongs the self-healing time. The area self-healing ratio, permeability, mechanical strength, precipitation depth method, numerical modeling, and ultrasonic method can be employed to identify the self-healing effect of cracks. Moreover, the self-healing mechanism is systematically analyzed. The results showed that microbial self-healing agents can repair cracks in cement-based materials in underground projects and dam gates. The difficulties and future development of self-healing cracks were analyzed. A microbial self-healing agent was embedded in the cement-based material, which automatically repaired the developing cracks. With the development of intelligent building materials, self-healing cracks have become the focus of attention.

关键词： cement-based materials     cracks     microbial self-healing agent     mechanism     intelligent building materials    

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Characterization of 3D microstructure, thermal conductivity, and heat flow of cement-based foam using

《结构与土木工程前沿（英文）》 2021年 第15卷 第3期   页码 643-651 doi: 10.1007/s11709-021-0709-9

摘要： This study presents the results of the 3D microstructure, thermal conductivity, and heat flow in cement-based foams and examines their changes with a range of densities. Images were captured using X-ray micro computed tomography (micro-CT) imaging technique on cement-based foam samples prepared with densities of 400, 600, and 800 kg/m3. These images were later simulated and quantified using 3D data visualization and analysis software. Based on the analysis, the pore volume of 11000 µm3 was determined across the three densities, leading to optimal results. However, distinct pore diameters of 15 µm for 800 kg/m3, and 20 µm for 600 and 400 kg/m3 were found to be optimum. Most of the pores were spherical, with only 10% appearing elongated or fractured. In addition, a difference of 15% was observed between the 2D and 3D porosity results. Moreover, a difference of 5% was noticed between the experimentally measured thermal conductivity and the numerically predicted value and this variation was constant across the three cast densities. The 3D model showed that heat flows through the cement paste solids and with an increase in porosity this flow reduces.

关键词： 3D pore volume distribution     X-ray tomography     3D shape factor     heat flow    

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Effect of surgical factors on the augmentation of cement-injectable cannulated pedicle screw fixationby a novel calcium phosphate-based nanocomposite

Haolin Sun, Chun Liu, Shunlun Chen, Yanjie Bai, Huilin Yang, Chunde Li, Lei Yang

《医学前沿（英文）》 2019年 第13卷 第5期   页码 590-601 doi: 10.1007/s11684-019-0710-z

摘要： Bone cement-augmented pedicle screw system demonstrates great efficacy in spinal disease treatments. However, the intrinsic drawbacks associated with clinically used polymethylmethacrylate (PMMA) cement demands for new bone cement formulations. On the basis of our previous studies, a novel injectable and biodegradable calcium phosphate-based nanocomposite (CPN) for the augmentation of pedicle screw fixation was systematically evaluated for its surgical feasibility and biomechanical performance by simulated and animal osteoporotic bone models, and the results were compared with those of clinical PMMA cement. ASTM-standard solid foam and open-cell foam models and decalcified sheep vertebra models were employed to evaluate the augmentation effects of CPN on bone tissue and on the cement-injected cannulated pedicle screws (CICPs) placed in osteoporotic bone. Surgical factors in CICPs application, such as injection force, tapping technique, screw diameter, and pedicle screw loosening scenarios, were studied in comparison with those in PMMA. When directly injected to the solid foam model, CPN revealed an identical augmentation effect to that of PMMA, as shown by the similar compressive strengths (0.73±0.04 MPa for CPN group vs. 0.79±0.02 MPa for PMMA group). The average injection force of CPN at approximately 40–50 N was higher than that of PMMA at approximately 20 N. Although both values are acceptable to surgeons, CPN revealed a more consistent injection force pattern than did PMMA. The dispersing and anti-pullout ability of CPN were not affected by the surgical factors of tapping technique and screw diameter. The axial pullout strength of CPN evaluated by the decalcified sheep vertebra model revealed a similar augmentation level as that of PMMA (1351.6±324.2 N for CPN vs. 1459.7±304.4 N for PMMA). The promising results of CPN clearly suggest its potential for replacing PMMA in CICPs augmentation application and the benefits of further study and development for clinical uses.

关键词： bone cement     pedicle screw     degenerative spinal diseases     calcium phosphate     injectable    

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Filtration ability of hollow fiber membrane for production of magnesium ammonium phosphate crystals by

H. Watamura, H. Marukawa, I. Hirasawa

《化学科学与工程前沿（英文）》 2013年 第7卷 第1期   页码 55-59 doi: 10.1007/s11705-013-1312-y

摘要： Relationship between magnesium ammonium phosphate (MAP) crystal properties and the filtration ability of hollow fiber membrane (HFM) were investigated. Phosphorus recovery process by crystallization has a problem that it produces a large amount of fine crystals. So improvement of the crystallization process by combining with filtration was discussed. MAP crystals were obtained by batch reaction crystallization and the filtration characteristics were investigated. The filtration was evaluated by the specific filtration resistance ( ) on HFM. Filtered slurry was prepared with each suspension density and crystal size distribution. The solution was filtered at constant pressure of 0.02 MPa and the filtration time on each filtrated volume was recorded. As a result, decreases exponentially with suspension density increasing from 0.25 g/L to 0.5 g/L and decreases moderately with suspension density increasing from 0.5 g/L to 1.5 g/L. of large crystals decreases exponentially at less suspension density than of small crystals does. Also, increases as the ratio of the fractured crystals increases.

关键词： membrane separation     crystallization     MAP    

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Cement-based solidification/stabilization of contaminated soils by nitrobenzene

Jianguo LIU, Xiaoqin NIE, Xianwei ZENG, Zhaoji SU

《环境科学与工程前沿（英文）》 2012年 第6卷 第3期   页码 437-443 doi: 10.1007/s11783-012-0406-y

摘要： The cement-based solidification/stabilization (S/S) of nitrobenzene (NB) contaminated soils, with cement and lime as binders, sodium silicate solution and powder activated carbon (PAC) as additives, was optimized through an orthogonal experiment, and S/S efficiency was estimated by both leaching test and volatilization measurement. The leaching test results showed that the factors affecting S/S efficiency were NB concentration, cement-to-lime ratio and binder-to-soils ratio, in sequence. With increasing curing time, the leaching concentration of NB between different levels of the same factor in the orthogonal experiment decreased, and less than 9% NB leached out from the 28 d cured samples. The volatilization measurement results indicated that 0.5‰ of NB was volatilized during the mixing and curing processes for the samples without PAC in the 28 d cycle, whereas adding 2 wt% and 5 wt% PAC, with respect to the weight of contaminated soils, could reduce NB volatilization to half of its original values either during the mixing or curing process. The optimizing formula, that is, contaminated soils (dry weight):cement:lime= 100:25:25, with 5 wt% additional sodium silicate and 2 wt% additional PAC, was applied to the engineering application of NB contaminated soils. Both the leaching test results of the product and the ambient air quality monitoring results met related regulations during the treating process.

关键词： solidification/stabilization     nitrobenzene     contaminated soils     powder activated carbon    

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Study of bond strength between various grade of Ordinary Portland Cement (OPC) and Portland PozzolaneCement (PPC) mixes and different diameter of TMT bars by using pullout test

A D POFALE, S P WANJARI

《结构与土木工程前沿（英文）》 2013年 第7卷 第1期   页码 39-45 doi: 10.1007/s11709-013-0193-y

摘要： Since last two decades, the Portland Pozzolane Cement (PPC) is extensively used in structural concrete. But, till to date, a few literature is available on bond strength of concrete using PPC mixes. There are many literatures available on bond strength of concrete mixes using Ordinary Portland Cement (OPC). Hence, a comparative study was conducted on bond strength between OPC and PPC mixes. In the present investigation, total 24 samples consisting of M20, M35 and M50 grades of concrete and 16 and 25 mm diameter of TMT bar were tested for 7 and 28 days. The pullout bond test was conducted on each specimen as per IS: 2770-1967/1997 [1] and the results were observed at 0.25 mm slip at loaded end called as critical bond stress and at maximum bond load called as maximum bond stress. It was observed that the critical bond strength of PPC mixes is 10% higher than OPC mixes. Whereas, marginal improvement was noticed in maximum bond strength of PPC mixes. Hence, based on these findings, it could be concluded that development length for PPC mixes could be reduced by 10% as compared with same grade of OPC mixes.

关键词： bond strength     Portland Pozzolane Cement (PPC) concrete     Ordinary Portland Cement (OPC) concrete     bond between concrete and steel     pullout test     development length    

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水泥基材料及其性能的分子模拟研究 Review

Ashraf A. Bahraq, Mohammed A. Al-Osta, Omar S. Baghabra Al-Amoudi, I.B. Obot,Mohammed Maslehuddin, Habib-ur-Rehman Ahmed, Tawfik A. Saleh

《工程（英文）》 2022年 第15卷 第8期   页码 165-178 doi: 10.1016/j.eng.2021.06.023

摘要：

Hydrated cement is one of the complex composite systems due to the presence of multi-scale phases with varying morphologies. Calcium silicate hydrate (C–S–H), which is the principal binder phase in the hydrated cement, is responsible for the stiffness, strength, and durability of Portland cement concrete. To understand the mechanical and durability behavior of concrete, it is important to investigate the interactions of hydrated cement phases with other materials at the nanoscale. In this regard, the molecular simulation of cement-based materials is an effective approach to study the properties and interactions of the cement system at the fundamental scale. Recently, many studies have been published regarding atomistic simulations to investigate the cement phases to define/explain the microscopic physical and chemical properties, thereby improving the macroscopic performance of hardened binders. The research in molecular simulation of cementitious systems involves researchers with multidisciplinary backgrounds, mainly in two areas: ① cement chemistry, where the hydration reactions govern most of the chemical and physical properties at the atomic scale; and ② computational materials science and engineering, where the bottom-up approach is required. The latter approach is still in its infancy, and as such, a study of the prevailing knowledge is useful, namely through an exhaustive literature review. This state-of-the-art report provides a comprehensive survey on studies that were conducted in this area and cites the important findings.

关键词： Atomistic simulation     Molecular dynamics     Cement phases     Hydration products     Nanoengineering    

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Experimental study and field application of calcium sulfoaluminate cement for rapid repair of concrete

Yanhua GUAN, Ying GAO, Renjuan SUN, Moon C. WON, Zhi GE

《结构与土木工程前沿（英文）》 2017年 第11卷 第3期   页码 338-345 doi: 10.1007/s11709-017-0411-0

摘要： The fast-track repair of deteriorated concrete pavement requires materials that can be placed, cured, and opened to the traffic in a short period. Type III cement and Calcium Sulfoaluminate (CSA) cement are the most commonly used fast-setting hydraulic cement (FSHC). In this study, the properties of Type III and CSA cement concrete, including compressive strength, coefficient of thermal expansion (CTE) and shrinkage were evaluated. The test results indicate that compressive strength of FSHC concrete increased rapidly at the early age. CSA cement concrete had higher early-age and long term strength. The shrinkage of CSA cement concrete was lower than that of Type III cement concrete. Both CSA and Type III cement concrete had similar CTE values. Based on the laboratory results, the CSA cement was selected as the partial-depth rapid repair material for a distressed continuously reinforced concrete pavement. The data collected during and after the repair show that the CSA cement concrete had good short-term and long-term performances and, therefore, was suitable for the rapid repair of concrete pavement.

关键词： Calcium Sulfoaluminate (CSA) cement     Type III cement     coefficient of thermal expansion (CTE)     shrinkage     rapid repair    

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Long term performance of recycled concrete beams with different water–cement ratio and recycled aggregate

Jingwei YING; Feiming SU; Shuangren CHEN

《结构与土木工程前沿（英文）》 2022年 第16卷 第3期   页码 302-315 doi: 10.1007/s11709-022-0803-7

摘要： The purpose of this study is to reveal the service performance of recycled aggregate concrete (RAC) components for different values of water−cement ratio and replacement rate of recycled coarse aggregate (RCA). Generally, the concrete strength decreases with the increase of the replacement rate of RCA, in order to meet the strength requirements when changing the replacement rate of RCA, it is necessary to change the water−cement ratio at the same time. Therefore, the axial compressive strengths of prism with 25 mix proportions, the short-term mechanical properties and long-term deformation properties of reinforced concrete beams were tested respectively by changing water−cement ratio and RCA replacement rate. The bearing capacity and the strain nephogram of samples under different loads were obtained using the Digital Image Correlation (DIC) method, and a self-made gravity loading experimental device was used for long-term deformation investigation. Results showed that the damage pattern of RAC was the same as that of natural aggregate concrete (NAC), but the brittleness was more pronounced. The brittleness of concrete before failure can be reduced more effectively by adjusting the replacement rate of RCA than by adjusting the water−cement ratio. The water−cement ratio has an evident influence on the axial compressive strength and early creep of concrete, while the replacement rate of RCA has a remarkable effect on the long-term deformation of the concrete beams.

关键词： recycled concrete     beam     the replacement rate of recycled coarse aggregate     water–cement ratio     digital image correlation    

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关于水泥混凝土发展方向的几点认识

唐明述

《中国工程科学》 2002年 第4卷 第1期   页码 41-46

摘要：

根据在加拿大观察到的重大混凝土工程破坏实例，反复强调我国在基建工程中必须十分重视耐久性问题。为实现可持续发展，应逐步将水泥工业转变为"绿色胶凝材料工业"。阐述了根据混凝土的技术进步重新审议水泥的标准与组成。最后建议把水泥的生产、流通与使用协调起来，以获得更大的经济和社会效益。

关键词： 水泥     混凝土     耐久性     分类     混合材     标准    

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标题 作者 时间 类型 操作

Experimental study on mechanical properties of a novel micro-steel fiber reinforced magnesium phosphatecement-based concrete

期刊论文

Autogenous healing mechanism of cement-based materials

期刊论文

Effect of size on biaxial flexural strength for cement-based materials by using a triangular plate method

Hakan T TURKER

期刊论文

Appraising the potential of calcium sulfoaluminate cement-based grouts in simulated permafrost environments

期刊论文

高性能多功能水泥基复合材料

Victor C. Li

期刊论文

Microbial self-healing of cracks in cement-based materials and its influencing factors

期刊论文

Characterization of 3D microstructure, thermal conductivity, and heat flow of cement-based foam using

期刊论文

Effect of surgical factors on the augmentation of cement-injectable cannulated pedicle screw fixationby a novel calcium phosphate-based nanocomposite

Haolin Sun, Chun Liu, Shunlun Chen, Yanjie Bai, Huilin Yang, Chunde Li, Lei Yang

期刊论文

Filtration ability of hollow fiber membrane for production of magnesium ammonium phosphate crystals by

H. Watamura, H. Marukawa, I. Hirasawa

期刊论文

Cement-based solidification/stabilization of contaminated soils by nitrobenzene

Jianguo LIU, Xiaoqin NIE, Xianwei ZENG, Zhaoji SU

期刊论文

Study of bond strength between various grade of Ordinary Portland Cement (OPC) and Portland PozzolaneCement (PPC) mixes and different diameter of TMT bars by using pullout test

A D POFALE, S P WANJARI

期刊论文

水泥基材料及其性能的分子模拟研究

Ashraf A. Bahraq, Mohammed A. Al-Osta, Omar S. Baghabra Al-Amoudi, I.B. Obot,Mohammed Maslehuddin, Habib-ur-Rehman Ahmed, Tawfik A. Saleh

期刊论文

Experimental study and field application of calcium sulfoaluminate cement for rapid repair of concrete

Yanhua GUAN, Ying GAO, Renjuan SUN, Moon C. WON, Zhi GE

期刊论文

Long term performance of recycled concrete beams with different water–cement ratio and recycled aggregate

Jingwei YING; Feiming SU; Shuangren CHEN

期刊论文

关于水泥混凝土发展方向的几点认识

唐明述

期刊论文